Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Tert-butyl-m-xylene → 2,6-Dimethyl-4-t-butyl-1-acryloylbenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Tert-butyl-m-xylene | HCID 7378 | — |
| 반응물 | Acryloyl chloride | HCID 13140 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 2,6-Dimethyl-4-t-butyl-1-acryloylbenzene | HCID 46913482 | — |
반응 단계
5-t-butylmetaxylene (0.5 mL), acryloyl chloride (120 mg), and aluminium chloride (150 mg) were reacted in dichloromethane (1.5 mL) at from −40° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (120 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08937091B2 |
| 출처 데이터셋 | uspto-grants-2015_01 |
| ORD ID | ord-1f38244b93d54d9a9df49f23e0d57e56 |
| 출처 메모 | uspto-grants-2015_01 |