Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1-Phenylnaphthalene → Acryloyl-1-phenylnaphthalene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1-Phenylnaphthalene | HCID 11795 | — |
| 반응물 | Acryloyl chloride | HCID 13140 | — |
| 반응물 | Aluminum(III) Chloride | HCID 6451240 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Acryloyl-1-phenylnaphthalene | HCID 86673232 | 125.2% |
반응 단계
1-phenylnaphthalene (204 mg), acryloyl chloride (200 mg), and aluminium chloride (290 mg) were reacted in dichloromethane (1.5 mL) at from −40° C. to room temperature for 2 hours. The resultant was treated in the same manner as described in Example 1 to obtain the title compound (323 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08937091B2 |
| 출처 데이터셋 | uspto-grants-2015_01 |
| ORD ID | ord-d3ef5e2ceed241289f186007c662443e |
| 출처 메모 | uspto-grants-2015_01 |