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HCID 68233453, 화합물 → (R,E)-4-Amino-5-phenylpent-2-enenitrile

HRID 1429407
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HRID 1429407 반응식
C(OC(=O)[NH:7][C@@H:8](/[CH:16]=[CH:17]/[C:18]#[N:19])[CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)(C)(C)C>Cl.CO>[NH2:7][C@H:8]([CH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)/[CH:16]=[CH:17]/[C:18]#[N:19]
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참가 물질

3

반응물 1

HCID 68233453HCID 68233453, 화합물

생성물 1

HCID 68233458(R,E)-4-Amino-5-phenylpent-2-enenitrile

시약·촉매·용매 1

HCID 21893726Hydrochloride methanol용매

실험 절차

Compound 31e (4.0 g, 14.7 mmol) was treated with 2M HCl/MeOH (300 mL). After the reaction was over, the solvents were removed under reduced pressure to give a white solid. The product was directly used in the next reaction step without further purification.

후처리

  1. customwere removed under reduced pressure
  2. customto give a white solid
  3. customThe product was directly used in the next reaction step without further purification

출처 및 근거

ORD 기록
ord-19eb24d404ee4e0ababa86f73d24d572
출처 데이터셋
uspto-grants-2015_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08940722B2

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