Ammonia → HCID 57417080, 화합물
반응식
C[O:2][C:3]([C@@H:5]1[CH2:9][C@@H:8]([N:10]([CH3:12])[CH3:11])[CH2:7][NH:6]1)=O.[NH3:13]>CO>[CH3:11][N:10]([CH3:12])[C@H:8]1[CH2:7][NH:6][C@H:5]([C:3]([NH2:13])=[O:2])[CH2:9]1참가 물질
4
실험 절차
A solution of (2S,4R)-4-Dimethylamino-pyrrolidine-2-carboxylic acid methyl ester (225 mg) and 7M ammonia in methanol (7 ml) is stood for 18 hours at room temperature in a sealed vessel. Evaporation and trituration with diethyl ether gives the title compound as a white solid.
후처리
- customEvaporation and trituration with diethyl ether
출처 및 근거
- ORD 기록
- ord-996118a1c14f4f54909fb351e4d91fee
- 출처 데이터셋
- uspto-grants-2015_01
- 특허 번호
- US08940771B2
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