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Methanol → Methyl cycloheptanecarboxylate

HRID 1430268
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HRID 1430268 반응식
[CH:1]1([C:8]([OH:10])=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.OS(O)(=O)=O.[CH3:16]O>>[CH:1]1([C:8]([O:10][CH3:16])=[O:9])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1
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참가 물질

4

반응물 3

HCID 887MethanolHCID 1118Sulfuric AcidHCID 15091Cycloheptanecarboxylic acid

생성물 1

HCID 543492Methyl cycloheptanecarboxylate

실험 절차

To a solution of 25.0 g cycloheptanecarboxylic acid in methanol (300 mL) was added concentrated H2SO4 (0.5 g) and the mixture was stirred at reflux overnight. The reaction mixture was concentrated under vacuum and the residue was diluted with ethyl ether (500 mL). The mixture was washed with water and brine, dried over Na2SO4, filtered, and concentrated under reduced pressure to give the title compound.

후처리

  1. temperatureat reflux overnight
  2. concentrationThe reaction mixture was concentrated under vacuum
  3. additionthe residue was diluted with ethyl ether (500 mL)
  4. washThe mixture was washed with water and brine
  5. dry with materialdried over Na2SO4
  6. filtrationfiltered
  7. concentrationconcentrated under reduced pressure

출처 및 근거

ORD 기록
ord-2691980ff03941ccbf4c3876102a151c
출처 데이터셋
uspto-grants-2015_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US08940737B2

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