Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodine chloride → 3-Chloro-4-amino-5-iodobenzylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodine chloride | HCID 24640 | — |
| 반응물 | 4-(Aminomethyl)-2-chloroaniline | HCID 21880650 | — |
| 용매 | Methanol | HCID 887 | — |
| 생성물 | 3-Chloro-4-amino-5-iodobenzylamine | HCID 58962991 | 42% |
반응 단계
To 3-Chloro-4-aminobenzylamine (200 mg, 1.28 mmol) in methanol (5 mL) was added iodine monochloride (230 mg, 1.42 mmol). The mixture was stirred for 1 hour, then purified by HPLC to give 3-chloro-4-amino-5-iodobenzylamine (150 mg, 42%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07612069B2 |
| 출처 데이터셋 | uspto-grants-2009_11 |
| ORD ID | ord-eede25dc32984281a7c2effb36f4b59a |
| 출처 메모 | uspto-grants-2009_11 |