Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Cyclohexen-1-one → 1,3-Diethyl 2-(3-oxocyclohexyl)propanedioate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Cyclohexen-1-one | HCID 13594 | — |
| 반응물 | 2-(3-Oxo-4-propylcyclohexyl)-malonic acid diethyl ester | HCID 57487436 | — |
| 생성물 | 1,3-Diethyl 2-(3-oxocyclohexyl)propanedioate | HCID 317049 | 88% |
반응 단계
Step 1 (3-Oxo-cyclohexyl)-malonic acid diethyl ester was prepared in 88% yield from cyclohexenone by the method described above for the synthesis of 2-(3-oxo-4-propylcyclohexyl)-malonic acid diethyl ester: 1H NMR (300 MHz, CDCl3) δ 4.44-4.12 (m, 4H), 2.88-1.22 (m, 16H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07727997B2 |
| 출처 데이터셋 | uspto-grants-2010_06 |
| ORD ID | ord-c7b90190713c40bf8958b5e59dd4121e |
| 출처 메모 | uspto-grants-2010_06 |