Methanol → Methyl 5-bromo-3-methylthiophene-2-carboxylate

HRID 1432776

반응식

S(Cl)(Cl)=O.[Br:5][C:6]1[S:10][C:9]([C:11]([OH:13])=[O:12])=[C:8]([CH3:14])[CH:7]=1.[CH3:15]O>>[Br:5][C:6]1[S:10][C:9]([C:11]([O:13][CH3:15])=[O:12])=[C:8]([CH3:14])[CH:7]=1

참가 물질

반응물 3

HCID 887Methanol

HCID 24386Thionyl Chloride

HCID 181766635-Bromo-3-methylthiophene-2-carboxylic acid

생성물 1

HCID 53438912Methyl 5-bromo-3-methylthiophene-2-carboxylate

실험 절차

After thionyl chloride was added to methanol, 5-bromo-3-methylthiophene-2-carboxylic acid was added thereto and the resulting solution was heated and refluxed to obtain methyl 5-bromo-3-methylthiophene-2-carboxylate. EI: 234, 236.

후처리

additionwas added
temperaturethe resulting solution was heated
temperaturerefluxed

출처 및 근거

ORD 기록: ord-ee3b2633ffc3488b8fc4da110dcdef8b
출처 데이터셋: uspto-grants-2009_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07612108B2

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