Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
5-Chloro-2-ethoxybenzoic acid → 2,4-Dichloro-6-(5-chloro-2-ethoxy-phenyl)-[1,3,5]triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 5-Chloro-2-ethoxybenzoic acid | HCID 5098570 | — |
| 반응물 | 2,4-Dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine | HCID 85827032 | — |
| 생성물 | 2,4-Dichloro-6-(5-chloro-2-ethoxy-phenyl)-[1,3,5]triazine | HCID 85827033 | 31% |
반응 단계
Using the method described for the synthesis of 2,4-dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine, 5-chloro-2-ethoxybenzoic acid afforded 2,4-dichloro-6-(5-chloro-2-ethoxy-phenyl)-[1,3,5]triazine (9.5 g, 31% yield). 1H NMR (DMSO-d6) 7.62-7.86 (m, 2H), 7.20-7.31 (m, 1H), 4.20 (m, 2H), 1.37 (m, 3H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07618968B2 |
| 출처 데이터셋 | uspto-grants-2009_11 |
| ORD ID | ord-0d9ef5c6beb446389066bdf434832052 |
| 출처 메모 | uspto-grants-2009_11 |