Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,5-Dichlorobenzoic acid → 2,4-Dichloro-6-(2,5-dichlorophenyl)-1,3,5-triazine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,5-Dichlorobenzoic acid | HCID 5784 | — |
| 반응물 | 2,4-Dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine | HCID 85827032 | — |
| 생성물 | 2,4-Dichloro-6-(2,5-dichlorophenyl)-1,3,5-triazine | HCID 20480386 | 14% |
반응 단계
Using the method described for the synthesis of 2,4-dichloro-6-(5-chloro-2-methyl-phenyl)-[1,3,5]triazine, 2,5-dichlorobenzoic acid afforded 2,4-dichloro-6-(2,5-dichloro-phenyl)-[1,3,5]triazine (2.2 g, 14% yield). 1H NMR (DMSO-d6) 8.10 (s, 1H), 7.50 (m, 2H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07618968B2 |
| 출처 데이터셋 | uspto-grants-2009_11 |
| ORD ID | ord-0e171e5dcf604b95ac974cec699bd988 |
| 출처 메모 | uspto-grants-2009_11 |