Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
7-(hydroxymethyl)-1H-pyrido[2,3-b][1,4]thiazin-2(3H)-one → 2-Oxo-2,3-dihydro-1h-pyrido[2,3-b][1,4]thiazine-7-carbaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 7-(hydroxymethyl)-1H-pyrido[2,3-b][1,4]thiazin-2(3H)-one | HCID 21873728 | — |
| 촉매 | HCID 178418406 | HCID 178418406 | — |
| 생성물 | 2-Oxo-2,3-dihydro-1h-pyrido[2,3-b][1,4]thiazine-7-carbaldehyde | HCID 21873733 | 58% |
반응 단계
7-Hydroxymethyl-1H-pyrido[2,3-b][1,4]thiazin-2-one (1.22 g) was oxidized with manganese dioxide by the method of Preparation (14c) to afford a solid (0.7 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07618959B2 |
| 출처 데이터셋 | uspto-grants-2009_11 |
| ORD ID | ord-6ee8c8a29da446ae8d6051bba5e25b35 |
| 출처 메모 | uspto-grants-2009_11 |