Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Silane, (chloromethyl)triethoxy- → 2-Propenoic acid, 2-methyl-, (triethoxysilyl)methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Silane, (chloromethyl)triethoxy- | HCID 84858 | — |
| 반응물 | Potassium methacrylate | HCID 23667354 | — |
| 촉매 | Phenothiazine | HCID 7108 | — |
| 촉매 | Tributylphosphine | HCID 13831 | — |
| 생성물 | 2-Propenoic acid, 2-methyl-, (triethoxysilyl)methyl ester | HCID 16225403 | 93.3% |
반응 단계
Using a method analogous to Example 4, 212.7 g (1 mol) of chloromethyltriethoxysilane are reacted in the presence of 11.1 g (0.03 mol) of tri-n-butylphosphine and 0.1 g of phenothiazine with 130.4 g (1.05 mol) of potassium methacrylate at 90° C. The reaction is complete 3 hours after all the potassium methacrylate has been introduced. Work-up gives 244.7 g (93%) of methacryloxymethyltriethoxysilane having a purity of 99.2%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07619108B2 |
| 출처 데이터셋 | uspto-grants-2009_11 |
| ORD ID | ord-49f1ff571b754eeda7e832166e4b363e |
| 출처 메모 | uspto-grants-2009_11 |