HCID 21400332, 화합물 → HCID 53991329, 화합물

HRID 1438704노트

반응식

HRID 1438704 반응식
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]([C:12](Cl)=[O:13])[C:9](Cl)=[O:10])=[CH:4][CH:3]=1.I.[CH3:16][S:17][C:18](=[NH:24])[NH:19][N:20]=[C:21]([CH3:23])[CH3:22]>C(N(CC)CC)C>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[C:12](=[O:13])[NH:24][CH:18]([S:17][CH3:16])[N:19]([N:20]=[C:21]([CH3:23])[CH3:22])[C:9]2=[O:10])=[CH:4][CH:3]=1

참가 물질

4

반응물 2

HCID 21400332HCID 21400332, 화합물HCID 178504061HCID 178504061, 화합물

생성물 1

HCID 53991329HCID 53991329, 화합물

시약·촉매·용매 1

HCID 8471Triethylamine용매

실험 절차

Analogously to Example 1, N-(4-chlorophenyl)-bis(chlorocarbonyl)-amine and acetone-S-methyl-isothiosemicarbazone hydroiodide with addition of triethylamine, yielded 1-(4-chlorophenyl)-3-isopropylideneamino-4-methylmercaptotetrahydro-1,3,5-triazine-2,6-dione as a colorless powder of melting point 142°-144° C.

출처 및 근거

ORD 기록
ord-5344c0a5dc71491a9e3bd00f09241cc0
출처 데이터셋
uspto-grants-1977_11
특허 번호
US04056527

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