Dichloromethane → HCID 13363448, 화합물
반응식
[CH3:1][N:2]([S:6]Cl)[C:3]([Cl:5])=[O:4].[CH2:8]([Cl:12])[C:9](=[CH2:11])[CH3:10].C(Cl)[Cl:14]>>[CH3:1][N:2]([S:6][C:9]([CH3:10])([CH2:11][Cl:14])[CH2:8][Cl:12])[C:3]([Cl:5])=[O:4]참가 물질
4
실험 절차
To a solution of 16.0g of N-methyl-N-chlorosulfenyl carbamoyl chloride in 100 ml of methylene chloride was added 12.0g of methallyl chloride with stirring, at room temperature. On slight heating there was a spontaneous exotherm which raised the temperature of the reaction mixture to 39° C. On removal of the solvent under reduced pressure 19.6g of oil was obtained.
후처리
- temperatureOn slight heating there
- temperatureraised the temperature of the reaction mixture to 39° C
- customOn removal of the solvent under reduced pressure 19.6g of oil
- customwas obtained
출처 및 근거
- ORD 기록
- ord-275fc3c3f7be489ba5023d54d6e54803
- 출처 데이터셋
- uspto-grants-1977_11
- 특허 번호
- US04058549
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