Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,3-Benzodioxole-5-carbonyl chloride → 1-Amino-3-[(1,1-dimethylethyl)(phenylmethyl)amino]propan-2-OL
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,3-Benzodioxole-5-carbonyl chloride | HCID 2734749 | — |
| 반응물 | 1-(3,4-methylenedioxy benzamido)-3-(N-benzyl tert-butylamino)-2-propanol hydrochloride | HCID 131710951 | — |
| 생성물 | 1-Amino-3-[(1,1-dimethylethyl)(phenylmethyl)amino]propan-2-OL | HCID 3016524 | 80% |
반응 단계
1-(3,4-methylenedioxy benzamido)-3-(N-benzyl tert-butylamino)-2- propanol hydrochloride, starting from 6.3 g (0.034 mole) of 3,4-methylenedioxy benzoyl chloride and 8 g (0.034 mole) of 1-amino-3-(N-benzyl tert-butylamino)-2- propanol (yield 80 %).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04059621 |
| 출처 데이터셋 | uspto-grants-1977_11 |
| ORD ID | ord-a4eacd56c26c4074825c045d053fe73e |
| 출처 메모 | uspto-grants-1977_11 |