Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → N-(2,2,6-trimethyl-2,3-dihydrobenzofuran-7-yl)hexadecaneamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Sodium Bicarbonate | HCID 516892 | — |
| 반응물 | Heptadecanoyl Chloride | HCID 3516438 | — |
| 반응물 | 7-Amino-2,2,6-trimethyl-2,3-dihydrobenzofuran | HCID 10607398 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-(2,2,6-trimethyl-2,3-dihydrobenzofuran-7-yl)hexadecaneamide | HCID 10835676 | — |
반응 단계
A 171 mg amount of hexadecanecarboxylic acid chloride was added to a solution of 100 mg of 7-amino-2,2,6-trimethyl-2,3-dihydrobenzofuran and 63 mg of triethylamine in 2 ml of dichloromethane, and the mixture was stirred at room temperature for one hour. A 10 ml amount of a saturated sodium hydrogencarbonate solution was added thereto, and the mixture was extracted twice with 20 ml of ethyl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05496853 |
| 출처 데이터셋 | uspto-grants-1996_03 |
| ORD ID | ord-b926b7ef2eaa4f22b4c8453c1d1c3211 |
| 출처 메모 | uspto-grants-1996_03 |