돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 1439929생성일: 2026년 10월 26일

Triethylamine → N-(2,2,6-trimethyl-2,3-dihydrobenzofuran-7-yl)hexadecaneamide

https://huagongshe.com/reaction/1439929

반응식

참여 물질

역할이름HCID투입량
반응물TriethylamineHCID 8471—
반응물Sodium BicarbonateHCID 516892—
반응물Heptadecanoyl ChlorideHCID 3516438—
반응물7-Amino-2,2,6-trimethyl-2,3-dihydrobenzofuranHCID 10607398—
용매DichloromethaneHCID 6344—
생성물N-(2,2,6-trimethyl-2,3-dihydrobenzofuran-7-yl)hexadecaneamideHCID 10835676—

반응 단계

A 171 mg amount of hexadecanecarboxylic acid chloride was added to a solution of 100 mg of 7-amino-2,2,6-trimethyl-2,3-dihydrobenzofuran and 63 mg of triethylamine in 2 ml of dichloromethane, and the mixture was stirred at room temperature for one hour. A 10 ml amount of a saturated sodium hydrogencarbonate solution was added thereto, and the mixture was extracted twice with 20 ml of ethyl acetate.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US05496853
출처 데이터셋uspto-grants-1996_03
ORD IDord-b926b7ef2eaa4f22b4c8453c1d1c3211
출처 메모uspto-grants-1996_03