Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydroquinone → Isodecyl methacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydroquinone | HCID 785 | — |
| 반응물 | Methyl Methacrylate | HCID 6658 | — |
| 반응물 | 4-Methoxyphenol | HCID 9015 | — |
| 반응물 | Dimethyltin dichloride | HCID 12955 | — |
| 반응물 | Isodecanol | HCID 32898 | — |
| 반응물 | Sodium Methoxide | HCID 10942334 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | Isodecyl methacrylate | HCID 34763 | 97.6% |
반응 단계
In a similar manner, 634.3 parts isodecyl alcohol, 603 parts methyl methacrylate, 220.6 parts heptane, 3.1 parts dimethyltin dichloride, 1.4 parts sodium methoxide (molar ratio 1.84:1) 2.21 parts 4-methoxyphenol and 0.73 parts hydroquinone were reacted as in Example 1 to yield 185.9 parts (97.6 percent yield, based on starting alcohol) of isodecyl methacrylate having a purity of 99.0 percent and containing no detectable tin.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05498751 |
| 출처 데이터셋 | uspto-grants-1996_03 |
| ORD ID | ord-df5ca9aca9c64748b0246b3f3da76a68 |
| 출처 메모 | uspto-grants-1996_03 |