Benzeneethanol, beta-methoxy- → 2-Methoxy-2-phenylethanal

HRID 1440875노트

반응식

HRID 1440875 반응식
[C:1]1([CH:7]([O:10][CH2:11]CC)[CH2:8][OH:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.COC(C1C=CC=CC=1)CO>>[C:1]1([CH:7]([O:10][CH3:11])[CH:8]=[O:9])[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1

참가 물질

3

반응물 2

HCID 102910Benzeneethanol, beta-methoxy-HCID 109868792-Phenyl-2-propoxyethanol

생성물 1

HCID 116439512-Methoxy-2-phenylethanal수율 69.8%

실험 절차

The procedure in Example 3 was repeated except that 180.25 g of 2-phenyl-2-propoxyethanol was replaced with 152 g of 2-methoxy-2-phenylethanol, to obtain 104.8 g of 2-phenyl-2-methoxyethanal (yield: 69%).

출처 및 근거

ORD 기록
ord-35f018865130441f94d67eb4f0ea27f9
출처 데이터셋
uspto-grants-1996_03
특허 번호
US05500484

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