Toluene → 2-Butoxy-2-phenylethanal

HRID 1440876노트

반응식

HRID 1440876 반응식
C1(C(OCCC)CO)C=CC=CC=1.[CH2:14]([O:18][CH:19]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[CH2:20][OH:21])[CH2:15][CH2:16][CH3:17].C1(C)C=CC=CC=1>C1CCCCC1>[CH2:14]([O:18][CH:19]([C:22]1[CH:27]=[CH:26][CH:25]=[CH:24][CH:23]=1)[CH:20]=[O:21])[CH2:15][CH2:16][CH3:17]

참가 물질

5

반응물 3

HCID 1140TolueneHCID 109868792-Phenyl-2-propoxyethanolHCID 143640482-Butoxy-2-phenylethanol

생성물 1

HCID 189826062-Butoxy-2-phenylethanal수율 68%

시약·촉매·용매 1

HCID 8078Cyclohexane용매

실험 절차

The procedure in Example 3 was repeated except that 180.25 g of 2-phenyl-2-propoxyethanol was replaced with 194 g of 2-butoxy-2-phenylethanol and 540 g of toluene was replaced with 580 g of cyclohexane, to obtain 130.5 g of 2-butoxy-2-phenylethanal (yield: 68%).

출처 및 근거

ORD 기록
ord-68d9cc76e0184287a214703db6e16b74
출처 데이터셋
uspto-grants-1996_03
특허 번호
US05500484

반응 노트

불러오는 중…