7380-79-2 → HCID 18982460, 화합물

HRID 1440888노트

반응식

HRID 1440888 반응식
[CH2:1]([B-:5]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)([C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[C:6]1[CH:11]=[CH:10][CH:9]=[CH:8][CH:7]=1)[CH2:2][CH2:3][CH3:4].[Li+].[Cl-].[CH3:26][S+:27]([CH3:37])[CH2:28]C(C1C=CC=CC=1)=O>O>[CH3:26][S+:27]([CH3:37])[CH2:28][C:18]1[CH:19]=[CH:20][CH:21]=[CH:22][CH:23]=1.[CH2:1]([B-:5]([C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1)([C:6]1[CH:7]=[CH:8][CH:9]=[CH:10][CH:11]=1)[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)[CH2:2][CH2:3][CH3:4]

참가 물질

4

반응물 2

HCID 218810807380-79-2HCID 23668465HCID 23668465, 화합물

생성물 1

HCID 18982460HCID 18982460, 화합물수율 181.8%

시약·촉매·용매 1

HCID 962Water용매2회

실험 절차

An aqueous solution of 10.11 g of lithium butyltriphenylborate in 100 ml of water was added to an aqueous solution of 6.24 g of dimethylphenacylsulfonium chloride in 150 ml of water, and the resultant mixture was stirred at room temperature for 30 minutes. The reaction mixture was filtered, and the resultant crystal was washed with water and dried to give 13.58 g of dimethylbenzylsulfonium-butyltriphenylborate as a white crystal.

후처리

  1. filtrationThe reaction mixture was filtered
  2. washthe resultant crystal was washed with water
  3. customdried

출처 및 근거

ORD 기록
ord-7fe3501b7f8c4eedb342298a10db1768
출처 데이터셋
uspto-grants-1996_03
특허 번호
US05500453

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