돌아가기
Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 14415생성일: 2026년 10월 24일

Hydrochloric Acid → 2-chloro-N-(3-chloroquinoxalin-2-yl)benzenesulfonamide

https://huagongshe.com/ko/reaction/14415

반응식

참여 물질

역할이름HCID투입량
반응물Hydrochloric AcidHCID 313—
반응물Potassium CarbonateHCID 11430—
반응물2,3-DichloroquinoxalineHCID 16659—
반응물2-ChlorobenzenesulfonamideHCID 81410—
용매WaterHCID 962—
용매DimethylformamideHCID 6228—
생성물2-chloro-N-(3-chloroquinoxalin-2-yl)benzenesulfonamideHCID 23122664101%

반응 단계

In the presence of potassium carbonate (625 mg), 2,3-dichloroquinoxaline (275 mg) and 2-chlorobenzenesulfonamide (264 mg) were allowed to react in the solution of dimethylformamide (4 mL) for 3 hours at 90° C. To the reaction mixture, water and hydrochloric acid were added and extracted with ethyl acetate. The residue was washed with a saturated aqueous solution of sodium chloride, dried with anhydrous magnesium sulfate and concentrated to obtain the title compound (493 mg) having the following physical data.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07732442B2
출처 데이터셋uspto-grants-2010_06
ORD IDord-f5faa8914f2c48cbb2a90c25cb447563
출처 메모uspto-grants-2010_06