2,3-Dichlorobenzene-1-sulfonyl chloride → 2,3-Dichloro-N-(5-chloro-3-methoxypyrazinyl)benzenesulfonamide
반응식
[Cl:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:11][C:12]1[C:17]([Cl:18])=[CH:16][CH:15]=[CH:14][C:13]=1[S:19](Cl)(=[O:21])=[O:20]>>[Cl:11][C:12]1[C:17]([Cl:18])=[CH:16][CH:15]=[CH:14][C:13]=1[S:19]([NH:8][C:5]1[C:4]([O:9][CH3:10])=[N:3][C:2]([Cl:1])=[CH:7][N:6]=1)(=[O:21])=[O:20]참가 물질
3
실험 절차
Prepared by the method of Example I (reaction performed at room temperature) using 5-chloro-3-methoxy-2-pyrazinamine (0.1 g) and 2,3-dichlorobenzenesulphonyl chloride (0.15 g). Yield 0.05 g.
후처리
- customPrepared by the method of Example I (reaction performed at room temperature)
출처 및 근거
- ORD 기록
- ord-7015e98d5cae45d1a4d8436c286072a7
- 출처 데이터셋
- uspto-grants-2010_02
- 특허 번호
- US07662825B2
반응 노트
불러오는 중…