3-Chlorobenzenesulphonyl chloride → 3-Chloro-N-(5-chloro-3-methoxy-2-pyrazinyl)benzenesulphonamide

HRID 1443973노트

반응식

HRID 1443973 반응식
[Cl:1][C:2]1[N:3]=[C:4]([O:9][CH3:10])[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:11][C:12]1[CH:13]=[C:14]([S:18](Cl)(=[O:20])=[O:19])[CH:15]=[CH:16][CH:17]=1>>[Cl:11][C:12]1[CH:13]=[C:14]([S:18]([NH:8][C:5]2[C:4]([O:9][CH3:10])=[N:3][C:2]([Cl:1])=[CH:7][N:6]=2)(=[O:20])=[O:19])[CH:15]=[CH:16][CH:17]=1

참가 물질

3

반응물 2

HCID 179093-Chlorobenzenesulphonyl chlorideHCID 107970362-Amino-5-chloro-3-methoxypyrazine

생성물 1

HCID 102152813-Chloro-N-(5-chloro-3-methoxy-2-pyrazinyl)benzenesulphonamide

실험 절차

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-chloro-3-methoxy-2-pyrazinamine (0.1 g) and 3-chlorobenzenesulphonyl chloride (0.13 g).

후처리

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

출처 및 근거

ORD 기록
ord-06287af46a1947d5ace9ef076e46a709
출처 데이터셋
uspto-grants-2010_02
특허 번호
US07662825B2

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