3-Chlorobenzenesulphonyl chloride → HCID 10126268, 화합물

HRID 1443981노트

반응식

HRID 1443981 반응식
[Cl:1][C:2]1[N:3]=[C:4]([O:10][CH3:11])[C:5]([NH2:9])=[N:6][C:7]=1[Cl:8].[Cl:12][C:13]1[CH:14]=[C:15]([S:19](Cl)(=[O:21])=[O:20])[CH:16]=[CH:17][CH:18]=1>>[Cl:12][C:13]1[CH:14]=[C:15]([S:19]([NH:9][C:5]2[C:4]([O:10][CH3:11])=[N:3][C:2]([Cl:1])=[C:7]([Cl:8])[N:6]=2)(=[O:21])=[O:20])[CH:16]=[CH:17][CH:18]=1

참가 물질

3

반응물 2

HCID 179093-Chlorobenzenesulphonyl chlorideHCID 179560285,6-Dichloro-3-methoxypyrazin-2-amine

생성물 1

HCID 10126268HCID 10126268, 화합물

실험 절차

Prepared by the method of Example 1 (reaction performed at room temperature) using 5,6-dichloro-3-methoxy-2-pyrazinamine (0.1 g) and 3-chlorobenzenesulphonyl chloride (0.13 g). Yield 0.047 g.

후처리

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

출처 및 근거

ORD 기록
ord-29519b5036e140688b911046a819f2fd
출처 데이터셋
uspto-grants-2010_02
특허 번호
US07662825B2

반응 노트

불러오는 중…