3-Chloro-2-methylbenzenesulfonyl chloride → HCID 10194699, 화합물

HRID 1444005노트

반응식

HRID 1444005 반응식
[Cl:1][C:2]1[N:3]=[C:4]([O:9][CH2:10][C:11]2[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=2)[C:5]([NH2:8])=[N:6][CH:7]=1.[Cl:17][C:18]1[C:19]([CH3:28])=[C:20]([S:24](Cl)(=[O:26])=[O:25])[CH:21]=[CH:22][CH:23]=1>>[Cl:17][C:18]1[C:19]([CH3:28])=[C:20]([S:24]([NH:8][C:5]2[C:4]([O:9][CH2:10][C:11]3[CH:12]=[N:13][CH:14]=[CH:15][CH:16]=3)=[N:3][C:2]([Cl:1])=[CH:7][N:6]=2)(=[O:26])=[O:25])[CH:21]=[CH:22][CH:23]=1

참가 물질

3

반응물 2

HCID 5227343-Chloro-2-methylbenzenesulfonyl chlorideHCID 59168203HCID 59168203, 화합물

생성물 1

HCID 10194699HCID 10194699, 화합물

실험 절차

Prepared by the method of Example 1 (reaction performed at room temperature) using 5-chloro-3-(3-pyridinylmethoxy)-2-pyrazinamine (Example 95a) (0.1 g) and 3-chloro-2-methylbenzenesulphonyl chloride (0.09 g). Yield 0.012 g.

후처리

  1. customPrepared by the method of Example 1 (reaction performed at room temperature)

출처 및 근거

ORD 기록
ord-f66c779101554490a310d8961c38e9ae
출처 데이터셋
uspto-grants-2010_02
특허 번호
US07662825B2

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