Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phenylmercuric Acetate → Phenyl acetate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phenylmercuric Acetate | HCID 16682730 | — |
| 반응물 | Phenyl iodoso diacetate | HCID 86738254 | — |
| 용매 | Acetic Acid | HCID 176 | — |
| 생성물 | Phenyl acetate | HCID 31229 | — |
반응 단계
The procedure of Example 3 is repeated except that only 10 ml. of acetic acid is charged to the reaction vessel, thereby increasing the concentration of the phenyl mercuric acetate and phenyl iodoso diacetate reactants in the liquid. At the end of the 0.25 hour of reaction at 120° C., phenyl acetate yield is found to be increased to 68%, at a phenyl mercuric acetate conversion of about 72% and a phenyl acetate selectivity of about 94%.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04316046 |
| 출처 데이터셋 | uspto-grants-1982_02 |
| ORD ID | ord-a28dddae7f5f4de8b751370c240c3100 |
| 출처 메모 | uspto-grants-1982_02 |