Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4'-Ethylacetophenone → 3-Dimethylamino-4'-ethylacrylophenone
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4'-Ethylacetophenone | HCID 13642 | — |
| 반응물 | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| 생성물 | 3-Dimethylamino-4'-ethylacrylophenone | HCID 53833899 | — |
반응 단계
A mixture of 50 g. of 4'-ethylacetophenone and 50 ml. of dimethylformamide dimethylacetal is refluxed for 16 hours. Evaporation gave a thick oil which crystallized on the addition of hexane, m.p. 80°-81° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04178449 |
| 출처 데이터셋 | uspto-grants-1979_12 |
| ORD ID | ord-63fd5dd7d8ac4491946c9a8f19e9106d |
| 출처 메모 | uspto-grants-1979_12 |