Sodium Carbonate → HCID 20376385, 화합물

HRID 1448452

반응식

HRID 1448452 반응식
[Br:1][C:2]1[CH:3]=[C:4]([CH:6]=[CH:7][C:8]=1[Br:9])[NH2:5].Cl.Cl[CH2:12][CH2:13][CH2:14][N:15]([CH3:17])[CH3:16].C(=O)([O-])[O-].[Na+].[Na+].C(=O)(O)[O-].[Na+]>C1(C)C=CC=CC=1>[CH3:16][N:15]([CH3:17])[CH2:14][CH2:13][CH2:12][NH:5][C:4]1[CH:6]=[CH:7][C:8]([Br:9])=[C:2]([Br:1])[CH:3]=1

참가 물질

6

반응물 4

HCID 10340Sodium CarbonateHCID 943083-(Dimethylamino)propyl chloride hydrochlorideHCID 516892Sodium BicarbonateHCID 5219813,4-Dibromoaniline

생성물 1

HCID 20376385HCID 20376385, 화합물

시약·촉매·용매 1

HCID 1140Toluene용매

실험 절차

In the manner given in Example 1, 3,4-dibromoaniline, 1-chloro-3-dimethylaminopropane hydrochloride, sodium carbonate and sodium bicarbonate are heated in toluene to give N,N-dimethyl-(3,4-dibromophenyl)trimethylenediamine.

출처 및 근거

ORD 기록
ord-7b901112f2594f4c9ed16c6daa437e49
출처 데이터셋
uspto-grants-1979_12
특허 번호
US04180522

연결된 노트

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