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llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
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HCID 20380305, 화합물 → HCID 20380311, 화합물

HRID 1448595
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인쇄 미리보기

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HRID 1448595 반응식
[ClH:1].C([N:9]1[CH2:14][CH:13]=[C:12]([C:15]2[C:21]([OH:22])=[CH:20][C:19]([CH:23]([CH3:25])[CH3:24])=[CH:18][C:16]=2[OH:17])[CH2:11][CH2:10]1)C1C=CC=CC=1.[H][H]>CO.[Pd]>[ClH:1].[NH:9]1[CH2:10][CH:11]=[C:12]([C:15]2[C:16]([OH:17])=[CH:18][C:19]([CH:23]([CH3:25])[CH3:24])=[CH:20][C:21]=2[OH:22])[CH2:13][CH2:14]1
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

5

반응물 2

HCID 20380305HCID 20380305, 화합물HCID 178418361HCID 178418361, 화합물

생성물 1

HCID 20380311HCID 20380311, 화합물수율 54.4%

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 887Methanol용매

실험 절차

The product of Example XI (30.1 g) was suspended in 150 ml methanol and hydrogenated using 4 g of 5% Pd on carbon. After uptake of 1 mole hydrogen, the catalyst was filtered, the solution concentrated and the residue crystallized from isopropyl alcohol to give 12.27 g (52.5%) of product, m.p. 269°-271°.

후처리

  1. concentrationthe solution concentrated
  2. customthe residue crystallized from isopropyl alcohol

출처 및 근거

ORD 기록
ord-0055b45d833c46bd95fdc42df5ffc172
출처 데이터셋
uspto-grants-1979_12
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04180669

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