반응식
CC(C(C)C=C)C=O.[CH3:9][C:10]([CH:15]([CH2:17][CH3:18])[CH3:16])([CH2:13][OH:14])[CH2:11][OH:12].C=O>>[CH3:9][C:10]([CH2:13][OH:14])([CH:15]([CH3:16])[CH:17]=[CH2:18])[CH2:11][OH:12]참가 물질
4
실험 절차
I have now found a novel method for producing mebutamate diol which includes the process steps of reacting crotyl alcohol and allyl chloride to produce a mixture of isomers of allyl crotyl ether, heating said crotyl ether to produce 2,3-dimethyl-pent-4en-aldehye. The aldehyde is then converted to 2-methyl-2-(sec butyl)-1, 3-propanediol by reacting 2,3-dimethyl-pent-4en-aldehyde and formaldehyde to produce 2,3-dimethyl-2-hydroxymethyl-pent-4en-ol and subsequently hydrogenating the said alcohol in the presence of a catalyst to produce 2-methyl-2-(sec butyl)-1,3-propanediol.
출처 및 근거
- ORD 기록
- ord-8143118e4cdb4b3c9f15d08d73cf9747
- 출처 데이터셋
- uspto-grants-1980_02
- 특허 번호
- US04190607
연결된 노트
불러오는 중…