3-(R)-(1-BOC-2-(S)-pyrrolidinyl)-4-nitrobutanol → 3-(R)-(1-BOC-pyrrolidin-2-(S)-yl)pyrrolidine
반응식
[C:1]([N:8]1[CH2:12][CH2:11][CH2:10][C@H:9]1[C@@H:13]([CH2:17][N+:18]([O-])=O)[CH2:14][CH2:15]O)([O:3][C:4]([CH3:7])([CH3:6])[CH3:5])=[O:2]>CO.[Pd]>[C:1]([N:8]1[CH2:12][CH2:11][CH2:10][C@H:9]1[C@@H:13]1[CH2:14][CH2:15][NH:18][CH2:17]1)([O:3][C:4]([CH3:7])([CH3:6])[CH3:5])=[O:2]참가 물질
4
실험 절차
The ether compound from step 471a was treated by hydrogenation at 4 atm H2 over Pd/C in methanol to give the tile compound.
후처리
- customto give the tile compound
출처 및 근거
- ORD 기록
- ord-0c8c306ab2af42f19a89b9d2eeb5fa2f
- 출처 데이터셋
- uspto-grants-1997_02
- 특허 번호
- US05599816
반응 노트
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