Benzyl Bromide → HCID 86749956, 화합물

반응식

[CH2:1]([O:3][CH:4]([C:8]1[N:9]([CH3:13])[CH:10]=[CH:11][N:12]=1)[O:5][CH2:6][CH3:7])[CH3:2].[CH2:14]([Br:21])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[Br-:21].[CH2:14]([N:12]1[CH:11]=[CH:10][N+:9]([CH3:13])=[C:8]1[CH:4]([O:3][CH2:1][CH3:2])[O:5][CH2:6][CH3:7])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

참가 물질

반응물 2

HCID 7498Benzyl Bromide

HCID 5741401H-Imidazole, 2-(diethoxymethyl)-1-methyl-

생성물 1

HCID 86749956HCID 86749956, 화합물수율 98.3%

실험 절차

A reaction mixture of 8 g (43 mmol) of 2-(diethoxymethyl-1-methyl-imidazole and 7.44 g (43 mmol) of benzyl bromide was stirred at room temperature overnight. The mixture was triturated with ethyl acetate and decanted to afford 15.1 g (98.3%) of 3-benzyl-2-(diethoxymethyl)-1-methylimidazolium bromide (Formula VI: A=1-methylimidazole; Y=CH(OC2H5)2 ; R1 =R6 =H; Z- =Br-).

후처리

customThe mixture was triturated with ethyl acetate
customdecanted

출처 및 근거

ORD 기록: ord-f4bef1d838794293a9c33cc6a524b7fe
출처 데이터셋: uspto-grants-1997_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05604224

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