참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Ethylhexanol | HCID 7720 | — |
| 반응물 | Ethyl (2-methylacryloyl)carbamate | HCID 13628540 | — |
| 촉매 | Hydroquinone | HCID 785 | — |
| 생성물 | 2-ethylhexyl N-methacryloylcarbamate | HCID 19973683 | 72.2% |
반응 단계
A reaction vessel was charged with 15.7 g of ethyl N-methacryloylcarbamate and 52 g of 2-ethylhexyl alcohol, to which 0.1 g of hydroquinone was added and heated at 120° C. for one hour. The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 17.4 g of 2-ethylhexyl N-methacryloylcarbamate having a viscosity of 800 cp.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05606096 |
|---|
| 출처 데이터셋 | uspto-grants-1997_02 |
|---|
| ORD ID | ord-db2484a96fec493cb3de5b738a92ebcb |
|---|
| 출처 메모 | uspto-grants-1997_02 |
|---|
