참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzylamine | HCID 7504 | — |
| 반응물 | Ethyl (2-methylacryloyl)carbamate | HCID 13628540 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | N-[(benzylamino)carbonyl]-2-methylacrylamide | HCID 639951 | 42.6% |
반응 단계
A reaction vessel was charged with 78.5 g of ethyl N-methacryloylcarbamate and 53.5 g of benzylamine to which 100 g of toluene were added and heated at 100° C. for 30 minutes, The resulting mixture was condensed under reduced pressure and isolated by column chromatography to obtain 46.4 g of N-benzyl-N'-methacryloyl urea having a melting point of 96°-98° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05606096 |
|---|
| 출처 데이터셋 | uspto-grants-1997_02 |
|---|
| ORD ID | ord-a8d45f9f89c844ebb793f09535acb143 |
|---|
| 출처 메모 | uspto-grants-1997_02 |
|---|
