Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methanesulfonylbenzene-1-sulfonyl chloride → HCID 178504719, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methanesulfonylbenzene-1-sulfonyl chloride | HCID 2735178 | — |
| 반응물 | HCID 178507363 | HCID 178507363 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | HCID 178504719 | HCID 178504719 | 82.4% |
반응 단계
N-(3-Iodo-1H-indazol-5-yl)-2-methylsulfonylbenzenesulfonamide can be obtained as described in Example 2 from 25.7 g of 5-amino-3-iodo-1H-indazole, 440 ml of pyridine and 25.3 g of 2-(methylsulfonyl)benzenesulfonyl chloride. 39 g of N-(3-iodo-1H-indazol-5-yl)-2-methylsulfonylbenzenesulfonamide are thus obtained in the form of a brown solid (mass analysis: Cl: m/z 478 (M+H)+, m/z 495 (M+NH4)+, m/z 260 (base peak)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07473701B2 |
| 출처 데이터셋 | uspto-grants-2009_01 |
| ORD ID | ord-aa174d0203294099a0a2428c685a01fd |
| 출처 메모 | uspto-grants-2009_01 |