3-Ethoxy-2-methylacrylaldehyde → HCID 178430151, 화합물

HRID 1453284

반응식

HRID 1453284 반응식
CCO/[CH:4]=[C:5](/[CH:7]=O)\[CH3:6].[NH2:9][C:10]1[N:14]=[C:13]([SH:15])[NH:12][N:11]=1>>[CH3:6][C:5]1[CH:4]=[N:9][C:10]2[N:11]([N:12]=[C:13]([SH:15])[N:14]=2)[CH:7]=1

참가 물질

3

반응물 2

HCID 30848683-Ethoxy-2-methylacrylaldehydeHCID 1785092965-amino-1H-1,2,4-triazole-3-thiol

생성물 1

HCID 178430151HCID 178430151, 화합물

실험 절차

The title compound was prepared from 3-ethoxymethacrolein and 3-amino-5-mercapto-1,2,4-triazole as previously described by M. Kunstlinger and E. Breitmaier in Synthesis, 1983, 44-47. 1H NMR (DMSO-d6) d 2.31 (s, 1H) 8.45 (s, 1H) 8.68 (s, 1H). MS (APCI) calcd for C6H6N4S: 166.21; found (M+H+) 167.0.

후처리

  1. customBreitmaier in Synthesis, 1983, 44-47

출처 및 근거

ORD 기록
ord-198a000b1b9648e1b5598f03f6cda602
출처 데이터셋
uspto-grants-2009_01
특허 번호
US07473790B2

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