Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methoxy-3-methylbenzoic Acid → 4-Methoxy-3-methyl-N-(1-pyridin-2-yl-butyl)-benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methoxy-3-methylbenzoic Acid | HCID 2759583 | — |
| 반응물 | 1-(Pyridin-2-yl)butan-1-amine | HCID 22767593 | — |
| 생성물 | 4-Methoxy-3-methyl-N-(1-pyridin-2-yl-butyl)-benzamide | HCID 57527755 | — |
반응 단계
Prepared in a similar manner to example 4 using 4-methoxy-3-methyl-benzoic acid and 1-pyridin-2-yl-butylamine. 1H NMR (500 MHz, CDCl3): δ 0.91-0.92 (t, 3H), 1.25-1.3 (m, 2H, 1.85-1.9 (m, 2H), 3.86 (s, 3H), 5.25-5.3 (m, 1H), 6.80-6.82 (d, 1H), 7.2-7.3 (m, 2H), 7.42-7.44 (d, 1H), 7.6-7.7 (m, 3H), 8.6 (d, 1H). MS (M+H, 299.1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07476399B2 |
| 출처 데이터셋 | uspto-grants-2009_01 |
| ORD ID | ord-a00939b1c64e406db73a7c6cdb5a6d36 |
| 출처 메모 | uspto-grants-2009_01 |