Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 5-bromo-6-nitro-2,3-dihydro-1H-inden-1-one
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 5-Bromo-1-indanone | HCID 520695 | — |
| 생성물 | 5-bromo-6-nitro-2,3-dihydro-1H-inden-1-one | HCID 53485149 | — |
반응 단계
Fuming nitric acid (166 ml) is cooled to −15° C., and 5-bromoindan-1-one (25 g, 0.118 mol) is then added portionwise. After stirring for 4 hours 30 minutes at between −10° C. and −15° C., the reaction mass is poured into ice-cold water (1600 ml).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07482484B2 |
| 출처 데이터셋 | uspto-grants-2009_01 |
| ORD ID | ord-1dc8686ba03a42cc8bf847e84f4e13de |
| 출처 메모 | uspto-grants-2009_01 |