Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 2-(Benzyloxy)-4-bromobenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Benzyl Bromide | HCID 7498 | — |
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | 4-Bromo-2-hydroxybenzaldehyde | HCID 4066019 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 2-(Benzyloxy)-4-bromobenzaldehyde | HCID 15673062 | — |
반응 단계
Benzyl bromide (1.35 ml) was added to a mixture of 4-bromo-2-hydroxybenzaldehyde (2.07 g) and potassium carbonate (1.38 g) in DMF (20 ml) and the mixture was stirred at ambient temperature for 10 hours. The reaction mixture was poured into water (50 ml) to give 2-benzyloxy-4-bromobenzaldehyde as a solid which was filtered and dried, yield 2.88 g. The material was used in subsequent reactions without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05843942 |
| 출처 데이터셋 | uspto-grants-1998_12 |
| ORD ID | ord-5240495585e14aebba79cf7818d27b88 |
| 출처 메모 | uspto-grants-1998_12 |