Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Phenyl-1-propanol → 2-(2-Phenylpropoxy)acetic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Phenyl-1-propanol | HCID 14295 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | tert-Butyl bromoacetate | HCID 79177 | — |
| 촉매 | Tetrabutylammonium Bromide | HCID 74236 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-(2-Phenylpropoxy)acetic acid | HCID 18779048 | 77.1% |
반응 단계
The subtitle compound (14.95 g) was prepared according to the procedure in example 6 part a using 2-phenyl-1-propanol (13.6 g), t-butylbromoacetate (19.5 g), tetrabutylammoniumbromide (3.2 g), toluene (70 ml), 50% aqueous sodium hydroxide (25 ml).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05846989 |
| 출처 데이터셋 | uspto-grants-1998_12 |
| ORD ID | ord-94dd09ff4c014c8f87066d566d816f84 |
| 출처 메모 | uspto-grants-1998_12 |