HCID 11107379, 화합물 → HCID 54135201, 화합물

반응식

[C:1]([O:4][CH2:5][C@@H:6]([C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][C:13]=1[O:20][CH3:21])[CH2:7][O:8]C(=O)C)(=[O:3])[NH2:2].C(OC[C@@H](C1C=CC=CC=1)COC(=O)C)(=O)N>>[C:1]([O:4][CH2:5][C@@H:6]([C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][C:13]=1[O:20][CH3:21])[CH2:7][OH:8])(=[O:3])[NH2:2]

참가 물질

반응물 2

HCID 11107379HCID 11107379, 화합물

HCID 67572920HCID 67572920, 화합물

생성물 1

HCID 54135201HCID 54135201, 화합물수율 65.3%

실험 절차

The title compound was synthesized in a similar manner to that of Example XXII, except that (S)-3-acetoxy-2-(2,4-dimethoxyphenyl)propanol carbamate, instead of (S)-3-acetoxy-2-phenylpropanol carbamate, was used as a starting material. Yield 65.3%. Purity 99.2%.

출처 및 근거

ORD 기록: ord-7195daf1741d4fbc984bf71b3b90ca55
출처 데이터셋: uspto-grants-1998_12
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US05849772

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