Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methyl iodide → N,N-diethyl 2-chloro-6-methylbenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methyl iodide | HCID 6328 | — |
| 반응물 | 2-Chloro-N,N-diethylbenzamide | HCID 82566 | — |
| 생성물 | N,N-diethyl 2-chloro-6-methylbenzamide | HCID 18630133 | 92% |
반응 단계
The compound from example e (1.0 eq) and MeI (3.0 eq) were combined according to Method A. The crude product was purified by HPLC with 1:4 EtOAc/hexanes to give 5.2 g of N,N-diethyl 2-chloro-6-methylbenzamide as a yellow solid, a 92% yield. m.p. 48°-49° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05849723 |
| 출처 데이터셋 | uspto-grants-1998_12 |
| ORD ID | ord-1a099b53b9b94e53a44f57914085fbd0 |
| 출처 메모 | uspto-grants-1998_12 |