Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-tert-Butylbenzyl alcohol → 4-t-Butylbenzyloxyoxalylchloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-tert-Butylbenzyl alcohol | HCID 13416 | — |
| 반응물 | Oxalyl chloride | HCID 65578 | — |
| 용매 | Diethyl Ether | HCID 3283 | — |
| 생성물 | 4-t-Butylbenzyloxyoxalylchloride | HCID 57118008 | — |
반응 단계
To a stirred solution of oxalyl dichloride (100ml) in diethylether (500 ml) at -10° under nitrogen a solution of 4-t-butylbenzyl alcohol (200 ml) in diethylether (100 ml) was added dropwise so as to maintain the temperature between -10° and -5°. The solvent was then evaporated under vacuum to give the title compound (289 g,) as a clear oil (b.p. 120°-122° at 2 mbar).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05849907 |
| 출처 데이터셋 | uspto-grants-1998_12 |
| ORD ID | ord-552cfa4c7d574c2cae876c5253dbc6fa |
| 출처 메모 | uspto-grants-1998_12 |