Ammonium Chloride → HCID 178439094, 화합물

HRID 1459201노트

반응식

HRID 1459201 반응식
CO[C:3]1[CH2:4][CH2:5][CH2:6][CH2:7][CH:8]([CH2:10][CH:11]=[CH2:12])[N:9]=1.[Cl-:13].[NH4+:14]>CO>[ClH:13].[CH2:10]([CH:8]1[NH:9][C:3](=[NH:14])[CH2:4][CH2:5][CH2:6][CH2:7]1)[CH:11]=[CH2:12]

참가 물질

4

반응물 2

HCID 25517Ammonium ChlorideHCID 107734033,4,5,6-Tetrahydro-7-methoxy-2-(2-propenyl)-2h-azepine

생성물 1

HCID 178439094HCID 178439094, 화합물수율 79.5%

시약·촉매·용매 1

HCID 887Methanol용매

실험 절차

The product of EXAMPLE 106 (70 mg, 0.42 mmol) in 3 mL of MeOH was reacted with ammonium chloride (21.4 mg, 0.4 mmol) by the method of EXAMPLE 27 to yield 60 mg (76%) of the title material.

출처 및 근거

ORD 기록
ord-93727c32a3a74cfa8533953e5163751d
출처 데이터셋
uspto-grants-1998_12
특허 번호
US05854234

반응 노트

불러오는 중…