Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitrobenzene → Dimethyl phenanthrene-3,4-dicarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitrobenzene | HCID 7416 | — |
| 반응물 | 2-Vinylnaphthalene | HCID 13230 | — |
| 반응물 | HCID 86613298 | HCID 86613298 | — |
| 생성물 | Dimethyl phenanthrene-3,4-dicarboxylate | HCID 15075419 | — |
반응 단계
A solution of 65 mmol of 2-vinylnaphthalene and 68 mmol of methyl acetylene-dicarboxylate in 200 ml of nitrobenzene is maintained at reflux for 14 hours. After distillation of the solvent, the reaction medium is chromatographed on silica (eluent: CH2Cl2) in order to obtain the expected product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05854273 |
| 출처 데이터셋 | uspto-grants-1998_12 |
| ORD ID | ord-c0fdf12d4df8490da35cb9ca2f64bf2e |
| 출처 메모 | uspto-grants-1998_12 |