Pyridine → HCID 15067105, 화합물

HRID 1460373노트

반응식

HRID 1460373 반응식
[CH2:1]([O:3][CH2:4][CH2:5][OH:6])[CH3:2].N1C=CC=CC=1.[S:13](Cl)([CH3:16])(=[O:15])=[O:14]>O1CCCC1>[CH3:16][S:13]([O:6][CH2:5][CH2:4][O:3][CH2:1][CH3:2])(=[O:15])=[O:14]

참가 물질

5

반응물 3

HCID 1049PyridineHCID 8076Glycol monoethyl etherHCID 31297Methanesulfonyl chloride

생성물 1

HCID 15067105HCID 15067105, 화합물

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

To 30g of 2-ethoxyethanol in 300ml of tetrahydrofuran 27.4ml of pyridine were added and 26.4ml of mesyl chloride added dropwise at room temperature over 15 minutes. The mixture was refluxed overnight, the solid that formed filtered off and the solvent evaporated off from the residue. The residue was distilled under 20m Hg to give 2-ethoxyethyl methanesulphonate.

후처리

  1. temperatureThe mixture was refluxed overnight
  2. customthe solid that formed
  3. filtrationfiltered off
  4. customthe solvent evaporated off from the residue
  5. distillationThe residue was distilled under 20m Hg

출처 및 근거

ORD 기록
ord-f8da1dc8ee6d42478c217b4800fba461
출처 데이터셋
uspto-grants-1991_12
특허 번호
US05071468

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