N-Phenylglycine → HCID 19100958, 화합물
반응식
[CH2:1]([N:4]([CH2:10][CH:11]=O)[C:5](=[O:9])[O:6][CH2:7][CH3:8])[CH:2]=[CH2:3].[C:13]1([NH:19][CH2:20]C(O)=O)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1>C1(C)C=CC=CC=1>[C:13]1([N:19]2[CH2:20][CH2:3][CH:2]3[CH:11]2[CH2:10][N:4]([C:5]([O:6][CH2:7][CH3:8])=[O:9])[CH2:1]3)[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1참가 물질
4
실험 절차
8.6 g (50 mmol) of ethyl N-allyl-N-(2-oxoethyl) -carbamate and 7.6 50 mmol) of phenylglycine are heated under reflux overnight in 200 ml of toluene. The mixture is decanted from resinous material and concentrated, and the residue is distilled.
후처리
- customThe mixture is decanted from resinous material
- concentrationconcentrated
- distillationthe residue is distilled
출처 및 근거
- ORD 기록
- ord-1fff63c7ccf74cd0a9ac9d39ead9c353
- 출처 데이터셋
- uspto-grants-1991_12
- 특허 번호
- US05071999
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