Water → Glycidoxypropyl Silanol

HRID 1461093

반응식

HRID 1461093 반응식
O.[CH2:2]([O:6][CH2:7][CH2:8][CH2:9][Si:10](OCC)(OCC)[O:11]CC)[CH:3]1[O:5][CH2:4]1>C(O)(=O)C>[CH2:2]([O:6][CH2:7][CH2:8][CH2:9][SiH2:10][OH:11])[CH:3]1[O:5][CH2:4]1

참가 물질

4

반응물 2

HCID 962WaterHCID 102856gamma-Glycidoxypropyltriethoxysilane

생성물 1

HCID 123537430Glycidoxypropyl Silanol

시약·촉매·용매 1

HCID 176Acetic Acid용매

반응 조건

온도
90 °C

실험 절차

In a three-necked flask equipped with a stirrer, dropping funnel and reflux condenser, 500 g water were adjusted with dilute acetic acid to a pH value of 4 to 4.5. 15 g glycidoxypropyl triethoxysilane were then added dropwise, the mixture being heated to 90° C. This temperature was maintained for 1 hour.

후처리

  1. customIn a three-necked flask equipped with a stirrer
  2. temperaturereflux condenser
  3. temperatureThis temperature was maintained for 1 hour

출처 및 근거

ORD 기록
ord-c4d35faa540c401f800b316ffa07cf99
출처 데이터셋
uspto-grants-1991_12
특허 번호
US05073588

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