Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → Fuming sulfuric acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | Pentachlorothiophenol | HCID 8620 | — |
| 반응물 | Sulfur trioxide | HCID 24682 | — |
| 반응물 | Sodium | HCID 5360545 | — |
| 생성물 | Fuming sulfuric acid | HCID 24681 | — |
반응 단계
reacting this sodium salt of pentachlorothiophenol with a mixed nitration acid comprising nitric acid and sulfuric acid (and, preferably, sulfur trioxide to form oleum) at a temperature from about 35° C. to about 110° C. to form pentachloronitrobenzene, the nitric acid being in molar excess of the pentachlorothiophenol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04461918 |
| 출처 데이터셋 | uspto-grants-1984_07 |
| ORD ID | ord-ef5d4417de7a4c94a97e21416b1302a2 |
| 출처 메모 | uspto-grants-1984_07 |