Methylamine → HCID 22851212, 화합물

HRID 1463547노트

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HRID 1463547 반응식
CO[C:3](=[O:14])[C@H:4]([CH2:6][C:7]1[CH:12]=[CH:11][C:10]([NH2:13])=[CH:9][CH:8]=1)[NH2:5].[CH3:15][NH2:16]>C(O)C>[CH3:15][NH:16][C:3](=[O:14])[C@H:4]([CH2:6][C:7]1[CH:8]=[CH:9][C:10]([NH2:13])=[CH:11][CH:12]=1)[NH2:5]

참가 물질

4

반응물 2

HCID 6329MethylamineHCID 206108304-Amino-L-phenylalanine methyl ester

생성물 1

HCID 22851212HCID 22851212, 화합물수율 100%

시약·촉매·용매 1

HCID 702Ethanol용매2회

실험 절차

To a stirred solution of p-aminophenylalanine methyl ester (1.7 g, 8.8 mmol) in ethanol (150 ml) was added methylamine in ethanol (33%/8M) (100 ml). After stirring at room temperature for 24 hours the reaction mixture was reduced under pressure to yield the title compound as a brown solid (1.7 g, 100%)

출처 및 근거

ORD 기록
ord-125e1dae273a4cdd924102ecc637f885
출처 데이터셋
uspto-grants-1994_04
특허 번호
US05300674

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